14MTET21 - Instrumenthal methods

Course specification
Course titleInstrumenthal methods
Study programme
Lecturer (for classes)
Lecturer/Associate (for practice)
    Lecturer/Associate (for OTC)
      ConditionОблик условљености
      The goalThe aim of the course is to provide students with theoretical knowledge about commonly used methods of chemical analysis, to instruct them how to choose the method for the analysis of different samples and to evaluate the reliability and accuracy of the chosen method.
      The outcomeStudents are expected to learn about the theoretical supposition on which the methods are based with an opportunity to apply these methods in chemical analysis of the real samples. In this course, students acquire knowledge on how to choose the method and perform the appropriate sample preparation, experimental measurements and the interpretation of results. The laboratory classes will help them to master the experimental technique.
      Contents of lecturesCalibration and standard solutions, Principles of spectral analysis, UV/Vis spectroscopy, Infrared spectroscopy, Fluorometry, Atomic absorption spectroscopy, Emission spectroscopy, Inductively coupled plasma, Gas chromatography, Liquid chromatography, Mass spectrometry, Nuclear magnetic resonance
      Contents of exercises1 Recording absorptive spectrum and determine the working wavelength ; 2 Quantitative determination of iron in water ; 3 Recording the infrared spectrum and identification of the compounds ; 4 Determination of zinc in water by atomic absorption spectroscopy ; 5 Quantitative analysis of mixtures of hydrocarbon gas chromatography ; 6 Liquid chromatography with ultraviolet detection ; 7 Mass Spectrometry ; 8 Inductivly coupled plasma using a mass - spectrometry detection ; 9 Liquid chromatography with mass - spectrometry detection
      1. F. Settle (Ed.), Hand Book of Instrumental Techniques for Analytical Chemistry, Prentice Hall Inc., New Jersey, 1997.
      2. L.D.Field, S.Sternhell, J.R.Kalman, Organic Structures from Spectra, John Wiley, 2002.
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      Number of hours per week during the semester/trimester/year
      LecturesExercisesOTCStudy and ResearchOther classes
      Methods of teachingThe classes are held through the lectures and experimental work in the laboratory.
      Knowledge score (maximum points 100)
      Pre obligationsPointsFinal examPoints
      Activites during lecturesTest paper50
      Practical lessons20Oral examination