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22ZP35 - Instrumental Methods

Course specification
Course titleInstrumental Methods
Acronym22ZP35
Study programmeBiochemical Engineering and Biotechnology
Module
Lecturer (for classes)
Lecturer/Associate (for practice)
    Lecturer/Associate (for OTC)
      ESPB3.0Status
      ConditionAnalytical Chemistry, Organic Chemistry IОблик условљености
      The goalThe aim of the course is to introduce commonly used instrumental methods of chemical analysis, to learn how to choose a method for analyzing different samples, and to evaluate the reliability and accuracy of the method chosen.
      The outcomeStudents are familiar with the theoretical backgrounds on which the methods are based, as well as with the possibilities of applying these methods in modern chemical analysis. In this course, students gain knowledge how to make a choice of the method, the proper preparation of the sample, the interpretation of the results, and through individual laboratory exercises they also master techniques of instrumentations.
      Contents
      Contents of lecturesCalibration and standard solutions, Principles of spectral analysis, Spectroscopy in the ultraviolet and visible region, Spectroscopy in the infrared region, Fluorimetry, Atomic absorption spectroscopy, Emission spectroscopy, Induction coupled plasma, Gas chromatography, Liquid chromatography, Liquid chromatography, Mass Spectrometry, NMR
      Contents of exercises1. Recording the absorption spectrum and determination of the operating wavelength 2. Quantification of iron in water 3. Infrared imaging and compound identification 4. Determination of zinc in water by atomic absorption spectroscopy 5. Quantitative analysis of the hydrocarbon mixture by gas chromatography 6. Liquid chromatography with ultraviolet detector 7. Mass spectrometry Combined methods (demonstration exercises) 8. Inductively coupled plasma with mass spectrometric detector 9. Liquid chromatography with mass spectrometric detector
      Literature
      1. Douglas A. Skoog, F. James Holler, Stanley R. Crouch, Principles of Instrumental Analysis, Cengage Learning 2018.
      2. James W. Robinson, Eileen Skelly Frame, George M. Frame II, Undergraduate Instrumental Analysis, CRC Press, 2014
      3. Graham Currel, Analytical Instrumentation, Wiley, 2010.
      4. S. Milosavljević, Strukturne instrumentalne metode, BU, Hemijski fakultet Beograd 1997. (Original title)
      5. D. Antonović, Instrumentalne metode u organskoj hemiji - zbirka zadataka, TMF, Beograd, 2003. (Original title)
      Number of hours per week during the semester/trimester/year
      LecturesExercisesOTCStudy and ResearchOther classes
      21
      Methods of teachingLectures (PPT presentation), Exercises.
      Knowledge score (maximum points 100)
      Pre obligationsPointsFinal examPoints
      Activites during lecturesTest paper40
      Practical lessons30Oral examination
      Projects
      Colloquia30
      Seminars