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22IIM33 - Materials characterization methods

Course specification
Course titleMaterials characterization methods
Acronym22IIM33
Study programmeMaterial Engineering
Module
Lecturer (for classes)
Lecturer/Associate (for practice)
    Lecturer/Associate (for OTC)
      ESPB5.0Status
      ConditionFor attendance: Fundamentals of materials engineering; for exam: The processing and application of ceramic materialsОблик условљености
      The goalThe aim of this course is to enable students to become familiar with the materials characterization methods as well as the commonly used instrumental methods of chemical analysis of materials. The aim is also to learn about the methods for monitoring the microstructural and the structural changes that occur during the processing of these materials.
      The outcomeThe course introduces to the students the basic methods for the characterization of materials and the raw materials and compounds for their synthesis. During the course, students will do the experimental exercise in the field of the materials characterization.
      Contents
      Contents of lecturesIntroduction to materials characterization methods, Principles of spectral analysis, UV-VIS spectroscopy, Atomic absorption spectroscopy, Inductively coupled plasma, Transmission and reflection FTIR analysis of materials, Raman analysis of materials, Material analysis by X-ray diffraction, Differential thermal methods of materials characterization, Thermogravimetric method for characterization of materials, Thermomicroscope for determining distribution and particle size, Surface area determination, Determination of pore size distribution, Scanning electron microscopy with EDS, Transmission electron microscopy, AFM, Examination of the microstructure of metal materials using light microscopy.
      Contents of exercisesAAS analysis of materials, FTIR analysis of materials, Material analysis by X-ray diffraction, Infrared spectroscopic analysis of materials, Thermomicroscope, DTA and TGA characterization, Determining of the distribution and size of particles, Determination of specific surface area, Scanning electron microscopy, EDS characterization methods, Transmission electron microscopy, AFM.
      Literature
      1. Đ.Janaćković, interne skripte, TMF.
      2. Lj. Karanović, Primenjena kristalografija, Univerzitet u Beogradu, 1996.
      3. Lj. Kostić-Gvozdenović, M.Todorović, R.Petrović, Praktikum iz tehnologije keramike, Univerzitet u Beogradu, Tehnološko-metalurški fakultet, Beograd, 2000.
      4. J. Mišović i T. Ast, Instrumentalne metode hemijske analize, TMF Beograd 1989.
      5. S. Milosavljević, Strukturne instrumentalne metode, BU, Hemijski fakultet Beograd 1997.
      Number of hours per week during the semester/trimester/year
      LecturesExercisesOTCStudy and ResearchOther classes
      31
      Methods of teachingLectures, practical lessons.
      Knowledge score (maximum points 100)
      Pre obligationsPointsFinal examPoints
      Activites during lecturesTest paper
      Practical lessons30Oral examination70
      Projects
      Colloquia
      Seminars