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22ZP21 - Analytical Chemistry

Course specification
Course titleAnalytical Chemistry
Acronym22ZP21
Study programmeBiochemical Engineering and Biotechnology,Environmental Engineering,Material Engineering,Metallurgical Enginering
Module
Lecturer (for classes)
Lecturer/Associate (for practice)
    Lecturer/Associate (for OTC)
      ESPB6.0Status
      ConditionGeneral Chemistry IОблик условљености
      The goalStudents should learn and adopt the theoretical basis of qualitative and quantitative chemical analysis, calculation of basic values ​​and parameters important for chemical analysis. The main objectives are: the application of the chemical equilibrium essential for chemical analysis; the application of theoretical knowledge to practical work in the laboratory (basic experimental techniques; preparing solutions, volumetric and gravimetric analysis, procedures and calculations).
      The outcomeThe main outcomes are the theoretical and practical knowledge for the qualitative and quantitative analysis of elements, ions and compounds in aqueous solutions. Training for the independent work concerning chemical analysis of different samples: water samples (the determination of basic physico-chemical parameters and cation and anion content), acids, bases, salt solutions, aqueous solutions with specific cations (metal-ions) and anions and also the samples representing industrial raw materials and products. Application of simple instrumental methods (measurement of pH values by potentiometric method).
      Contents
      Contents of lecturesThe essence, major principles and the application of analytical chemistry. Qualitative chemical analysis. Principles, techniques, and basic operations in qualitative chemical analysis. Quantitative chemical analysis. Principles, techniques, and basic operations in quantitative chemical analysis. Chemical equilibrium in homogeneous and heterogeneous systems Principles of gravimetric analysis (separation methods and the determinition of ions in aqueous solutions). Principles of volumetric analysis (basic operations and techniques for the determination of ions in aqueous solutions). Acid-base titrations. Precipitation titrations. Complexometric titrations. Redox titrations. Application of classical methods in the analysis of real samples.
      Contents of exercisesTen independent laboratory experiments (10 LE). Identification of cations classified in V analytical groups. Identification of anions. Gravimetric analysis (determination of ions concentration in aqueous solutions). Volumetric analysis (determination of ion concentration in aqueous solutions). Neutralization, complexometric, precipitation and redox titrations for determination of content acids, bases and salts in aqueous solutions. Determination of the mass fraction of element in solid samples. Instrumental analysis (potentiometry-the determination of pH values).
      Literature
      1. Lj. Rajaković, Analytical Chemistry-Qualitative Chemical Analysis, Laboratory manuel with problems, tests and solutions, TMF, Belgrade, 2003, 2018
      2. Lj.Rajaković, A.Perić-Grujić, T.Vasiljević, D.Čičkarić-Živojinović, Analytical chemistry-quantitative chemical analysis, Laboratory manuel with theoretical aspects, TMF, Belgrade, 2000, 2004, 2010, 2018
      3. Lj. Rajaković, Analytical Chemistry-Problems and Solutions, TMF, Belgrade, 2005, 2013
      4. D. Skoog, D. West, J. Holler, S. Crouch, Fundamentals of Analytical Chemistry, 9th ed., Brooks/Cole, Belmont, CA, USA, 2013.
      5. R.Kellner, Analytical Chemistry-A Modern Approach to Analytical Science, John Wiley & Sons, New York, 2004
      Number of hours per week during the semester/trimester/year
      LecturesExercisesOTCStudy and ResearchOther classes
      33
      Methods of teachingTeaching methods: Lectures (classical methodology, power point (PPT) presentations), testing (3), colloquia (2). Experimental individual work in the lab (10).
      Knowledge score (maximum points 100)
      Pre obligationsPointsFinal examPoints
      Activites during lectures5Test paper50
      Practical lessons10Oral examination
      Projects
      Colloquia35
      Seminars